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41.
Susan C. Scott Nicole M. Anders Ping He Avelina Hemingway Steven D. Gore Christine L. Hann Michelle A. Rudek 《Biomedical chromatography : BMC》2022,36(3):e5289
The Bcl-2 family small molecule inhibitor navitoclax is being clinically evaluated to treat multiple cancers including lymphoid malignancies and small cell lung cancer. A sensitive and reliable method was developed to quantitate navitoclax in human plasma using liquid chromatography with tandem mass spectrometry with which to perform detailed pharmacokinetic studies. Sample preparation involved protein precipitation using acetonitrile. Separation of navitoclax and the internal standard, navitoclax-d8, was achieved with a Waters Acquity UPLC BEH C18 column using isocratic flow over a 3 min total analytical run time. A SCIEX 4500 triple quadrupole mass spectrometer operated in positive electrospray ionization mode was used for the detection of navitoclax. The assay range was 5–5,000 ng/ml and proved to be accurate (89.5–104.9%) and precise (CV ≤ 11%). Long-term frozen plasma stability for navitoclax at −70°C was at least 43 months. The method was applied for the measurement of total plasma concentration of navitoclax in a patient receiving a 250 mg daily oral dose. 相似文献
42.
Chemistry of Natural Compounds - 相似文献
43.
Vasile M. Loots H. Vercammen L. Bruggeman M. Verrezen F. 《Journal of Radioanalytical and Nuclear Chemistry》2022,331(8):3349-3357
Journal of Radioanalytical and Nuclear Chemistry - In this paper a study for the selection of an NPE (nonylphenol ethoxylates)—free cocktail is discussed in order to be used for our routine... 相似文献
44.
Yang T. L. Kao C. L. Kuo C. E. Yeh H. C. Li W. J. Li H. T. Chen C. Y. 《Chemistry of Natural Compounds》2022,58(5):825-827
Chemistry of Natural Compounds - A novel bibenzyl derivative, hydrangchinenin (1), was isolated from the stems of Hydrangea chinensis Maxim. (Hydrangeaceae). Its structure was determined on the... 相似文献
45.
46.
Tsvetkov D. S. Mazurin M. O. Sereda V. V. Ivanov I. L. Malyshkin D. A. Zuev A. Yu. 《Journal of Thermal Analysis and Calorimetry》2022,147(22):12661-12667
Journal of Thermal Analysis and Calorimetry - The results of thermochemical study of the CsPbCl3 formation thermodynamics available in literature were critically evaluated by comparison with those... 相似文献
47.
Journal of Analytical Chemistry - We review the main techniques, procedures, and information products used in non-target analysis (NTA) to reveal the composition of substances. Sampling and sample... 相似文献
48.
Filatova S. M. Guseva M. K. Bodrova T. G. Parshina D. V. Budanova U. A. Sebyakin Yu. L. 《Russian Journal of General Chemistry》2022,91(1):S13-S23
Russian Journal of General Chemistry - The review article traces the main trends of the synthetic approach to the solution of the problem of overcoming the resistance of pathogenic bacterial... 相似文献
49.
Sizova N. L. Golovina T. G. Konstantinova A. F. Dudka A. P. 《Crystallography Reports》2021,66(6):1045-1050
Crystallography Reports - The anisotropy of microhardness and fracture of the (0001) basal plane of langasite crystal has been studied using Berkovich indentation under a load of 100 g at different... 相似文献
50.
Physics of the Solid State - Local internal stresses in two natural inhomogeneous materials differing in the structure have been calculated using analysis of pauses between acoustic emission... 相似文献